COPPER (II) OXIDE, IS AN IMPORTANT P-TYPE SEMICONDUCTOR OXIDE WITH A VALUABLE INDUSTRIAL MATERIAL WITH MANY PROPERTIES SUCH AS ELECTRICAL, OPTICAL AND SO ON. UP TO DATE, CUO WITH DIFFERENT MORPHOLOGIES HAVE BEEN SUCCESSFULLY SYNTHESIZED BY VARIOUS TECHNIQUES [1]. ONE OF THE APPROACHES TO PREPARE CUPRIC OXIDE NANOSTRUCTURES IS THE BALL MILLING OR MECHANOCHEMICAL METHOD [2]. IN FACT, MECHANICAL MILLING IS AN EFFECTIVE, USEFUL, LOW-COST AND A SIMPLE TECHNIQUE, WHICH IS USED TO SYNTHESIZE NUMEROUS MATERIALS [3]. IN THIS WORK, WE SYNTHESIZED CUO IN NANO SCALE BY UTILIZING MECHANOCHEMICAL REACTION AND THEN CALCINATION PROCEDURE. COPPER ACETATE MONOHYDRATE AND ACE TAMIDE WERE USED AS REAGENTS AND THE RESULTING PRECURSOR WAS CALCINATED AT 350 OC FOR 2H IN AIR. ALSO, WE INVESTIGATED THE INFLUENCE OF THE BALL MILLING TIME ON THE MORPHOLOGY OF THE OBTAINED CUO. THE BEST MORPHOLOGY, NANOWIRES, OBTAINED WITH 50 MINUTE BALL MILLING (FIG. 1). THE PRODUCT WAS CHARACTERIZED BY USING FT–IR, XRD AND SEM TECHNIQUES.